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2016

Structural Aspects of Solid Solutions of Enantiomers (review) C. Brandel, S. Petit, Y. Cartigny, G. Coquerel Curr. Pharm. Des., 2016, in press

Review on micro-gas analyser systems: feasibility, separations and applications E. Lussac, R. Barattin, P. Cardinael, V. Peulon-Agasse (review) Crit. Rev. Anal. Chem. 2016, in press

Transformation of an active pharmaceutical ingredient upon high-energy milling: A process-induced disorder in Biclotymol B. Schammé, N. Couvrat, P. Malpeli, E. Dudognon, L. Delbreilh, V. Dupray, É. Dargent, G. Coquerel Int. J. Pharm., 2016, 499, 67-73

Evidence of Two Types of Fluid Inclusions in Single Crystals E. Bobo, B. Lefez, M.-C. Caumon, S. Petit, G. Coquerel
CrystEngComm, 2016, in press, DOI: 10.1039/C6CE00956E

Self-assembled -conjugated organic nanoplates: from hexagonal to triangular motifs D. E. Martínez, G. Gbabode, C. Ruzié, B. Chattopadhyay, G. Schweicher, A. R. Kennedy, Y. H. Geerts, M. Sferrazza RSC Adv. 2016, 6, 44921-44931

Partial Blockage of the Reversible Solid-Solid Transition of Strontium Succinate N. Couvrat, D. Martins, A. Lafontaine, M. Sanselme, V. Dupray, P. Taulelle, J.-M. Lerestif, M. Lynch, L. Vaysse-Ludot, G. Coquerel Chem. Eng. Technol., 2016, 38 (6), 999-1005

Crystal Structures and Phase Relationships of 2 Polymorphs of 1,4-Diazabicyclo[3.2.2]nonane-4-Carboxylic Acid 4-Bromophenyl Ester Fumarate, A Selective α-7 Nicotinic Receptor Partial Agonist B. Robert, M. -A. Perrin, M. Barrio, J.-L. Tamarit, G. Coquerel, R. Céolin, I. B. Rietveld J. Pharm. Sci., 2016, 105, 64-70

Access to Several Polymorphic Forms of (±)-Modafinil by Using Various Solvation–Desolvation Processes J. Mahieux, M. Sanselme, G. Coquerel Cryst. Growth Des., 2016, 16 (1), 396-405

The topological pressure-temperature phase diagram and crystal structures of the dimorphic system spiperone B. Robert, M. -A. Perrin, M. Barrio, J-L. Tamarit, G. Coquerel, R. Céolin, I. B. Rietveld Annales Pharmaceutiques Françaises, 2016, 74 (2), 129-136

Enantiomerisation of allylic trifluoromethyl sulfoxides studied by HPLC analysis and DFT calculations L. Bailly, E. Petit, M. Maeno, N. Shibata, O. Trapp, P. Cardinael, I. Chataigner, D. Cahard Chirality, 2016, 28 (2), 136-142

Evaluation of thermally pretreated silica stationary phases under hydrophilic interaction chromatography conditions M. Mignot, A. Périat, V. Peulon-Agasse, P. Cardinael, J.-L. Veuthey, D. Guillarme J. Sep. Sci., 2016, 39 (9), 1611-1618


Phenanthrene Purification: Comparison of Zone Melting and Co-Crystallization A. Burel, S.J.T. Brugman, M. Mignot, Y. Cartigny, S. Tisse, N. Couvrat, V. Peulon‐Agasse, P. Cardinael, G. Coquerel Chem. Eng. Technol., 2016, 39 (DOI: 10.1002/ceat.201600033)

Precise Urea/Water Eutectic Composition by Temperature-Resolved Second Harmonic Generation L. Yuan, S. Clevers, N. Couvrat, Y. Cartigny, V. Dupray, G. Coquerel Chem. Eng. Technol., 2016, 39, (DOI: 10.1002/ceat.201600032)

Trimorphism of N-methylurea : crystal structures, phase transitions and thermodynamic stabilities G. Baaklini, G. Gbabode, S. Clevers, P. Negrier, D. Mondieig, G. Coquerel CrystEngComm, 2016, in press (DOI: 10.1039/C6CE00652C)

Construction of Chiral Polar Crystals from Achiral Molecules by Stacking Control of Hydrogen-bonded Layers Using Type II Halogen Bonds T. Sasaki, Y. Ida, I. Hisaki, S. Tsuzuki, N. Tohnai, G. Coquerel, H. Sato, M. Miyata Cryst. Growth Des., 2016, 16 (3), 1626-1635

A kinetic/thermodynamic origin of regular chiral fluctuation or symmetry breaking unique toPreferential Enrichment Y. Uchida, S. Iwama, G. Coquerel, R. Tamura Chem. Eur. J., 2016, in press

Pre-Nucleation Self-Assembly and Chiral Discrimination Mechanisms during Solution Crystallization of Racemic Diprophylline C. Brandel, Y. Cartigny, G. Coquerel, J. H.t Horst, S. Petit Chem. Eur. J., 2016, submitted 

2015

Solubility of chiral species as function of the enantiomeric excess (review) G. Coquerel J. Pharm. Pharmacol., 2015, 67, 869–878

Formation of New Polymorphs Without any Nucleation Step. Desolvation of the Rimonabant Monohydrate: Directional Crystallisation Concomitant to Smooth Dehydration B. Fours, Y. Cartigny, S Petit, G. Coquerel Faraday Discussions 2015, 179, 475-488

Measuring Induction Times and Crystal Nucleation Rates C. Brandel, J.H. ter Horst Faraday Discussions 2015, 179, 199-214

Naproxen −Nicotinamide Cocrystals: Racemic and Conglomerate Structures Generated by CO2 Antisolvent Crystallization C. Neurohr, M. Marchivie, S. Lecomte, Y. Cartigny, N. Couvrat, M.Sanselme, P. Subra-Paternault Cryst. Growth Des., 2015, 15, 4616-4626

Structural characterization of a [1]benzothieno[3,2- b ]benzothiophene (btbt) derivative in bulk and thin films G. Gbabode, A. Blangenois,·P. Négrier, D. Mondieig,·G. Coquerel, Y. Geerts,·M. Sferrazza Acta Crystallographica, 2015,A71(a1):s514-s514

Enhanced Second Harmonic Generation from an Organic Self-Assembled Eutectic Binary Mixture: A Case Study with 3‑Nitrobenzoic and 3,5-Dinitrobenzoic Acids F. Simon, S. Clevers, G. Gbabode, N. Couvrat, V. Agasse-Peulon, M. Sanselme, V. Dupray, G. Coquerel. Cryst. Growth Des. 2015, 15, 946−960

Naproxen−Nicotinamide Cocrystals: Racemic and Conglomerate Structures Generated by CO2 Antisolvent Crystallization. C. Neurohr, M. Marchivie, S. Lecomte, Y. Cartigny, N. Couvrat, M.Sanselme, P. Subra-Paternault Cryst. Growth Des., 2015, 15, 4616-4626

Inhibition of the spontaneous polymorphic transition of pyrazinamide γ form at room temperature by co-spray drying with 1,3-dimethylurea. G. Baaklini, V. Dupray, G. Coquerel. Int. J. Pharm., 2015, 479, 163-170.

Simple access to highly functional bicyclic g- and d-lactams: origins of chirality transfer to contiguous tertiary/quaternary stereocenters assessed by DFT. R. Le Goff, A. Martel, M. Sanselme, A. Martin Lawson, A. Daïch, S. Comesse. Chem. Eur. J., 2015, 21 (7), 2966-2979

Formation of New Polymorphs without any Nucleation Step. Desolvation of the Rimonabant Monohydrate: Directional Crystallisation Concomitant to Smooth Dehydration.  B. Fours, Y. Cartigny, S Petit, G. Coquerel. Faraday Discuss. 2015, 179, 475-488

Measuring Induction Times and Crystal Nucleation Rates. C. Brandel, J.H. Ter Horst. Faraday Discuss. 2015

Crystallization of Terutroban Sodium Salt Hydrate from the Deliquescent State. N. Couvrat, Y. Cartigny, J. Linol, L. Vaysse-Ludot, P. Langlois, G. Coquerel. Chem. Eng. Technol., 2015, 38, 999-1005

Growth rate dispersion at single crystal level. E. Bobo, S. Petit, G. Coquerel. Chem. Eng. Technol., 2015

Ultrasound-Enhanced Deracemization: Towards the Existence of Agonist Effects in the Interpretation of Spontaneous Symmetry Breaking. C. Rougeot, F. Guillen, J-C. Plaquevent, G. Coquerel. Cryst. Growth Des., 2015, 15, 2151-5155

Relevance of Second Harmonic Generation (SHG) in Crystallization Processes. F.Simon, S. Clevers, V. Dupray, G. Coquerel. Chem. Eng. Technol., 2015, 38, 971-983

Review on ‘Solubility of chiral species as function of the enantiomeric excess’. G. Coquerel. J. Pharm. Pharmacol., 2015, 67, 869–878

Deracemisation of 2-Fluorophenylglycine by Attrition Induced Grinding. P. Wilmink, C. Rougeot, K. Wurst, M. Sanselme, M. van der Meijden, W. Saletra, G. Coquerel, R. M. Kellogg Org. Proc. Res. Dev., 2015, 19(1), 302-308

Crystallization kinetics and molecular mobility of an amorphous active pharmaceutical ingredient: A case study with Biclotymol. B. Schammé, N. Couvrat, P. Malpeli, L. Delbreilh, V. Dupray, E. Dargent, G. Coquerel. Int. J. Pharm., 2015; 490, 248-257

Mechanisms of Reversible Phase Transitions in Molecular Crystals: Case of Ciclopirox. C. Brandel, Y. Cartigny, N. Couvrat, E. Eusébio; J. Canotilho; S. Petit, G. Coquerel.Chemistry of Materials Accepted September 2015

Polymorphism of dioctyl-terthiophene within thin films: the role of the first monolayer. C. Lercher, C. Röthel, O. M. Roscioni, Y. H. Geerts, Q. Shen, C. Teichert, R. Fischer, G. Leising, M. Sferrazza, G. Gbabode, R. Resel. Chem. Phys. Lett., 2015, DOI:10.1061/j.cplett.2015.04.027 (in press)

Thermal pretreatments of superficially porous silica particles for high-performance liquid chromatography: Surface control, structural characterization and chromatographic evaluation. M. Mignot, M. Sebban, A. Tchapla, O. Mercier, P. Cardinael, V. Peulon-Agasse J. Chromatogr. A, 2015, 1419, 45-57

Enantiomerisation of allylic trifluoromethyl sulfoxides studied by HPLC analysis and DFT calculations. L. Bailly, E. Petit,[a] M. Maeno, N. Shibata, O. Trapp, P. Cardinael, I. Chataigner, D. Cahard Chirality, 2015 in press.

Comparison of cryogenic and differential flow (forward and reverse fill/flush) modulators and applications to the analysis of heavy petroleum cuts by High Temperature Comprehensive Gas Chromatography. C. Duhamel, P. Cardinael, V. Peulon-Agasse, R. Firor, L. Pascaud, G. Semard-Jousset, P. Giusti, V. Livadaris J. Chromatogr. A, 2015, 1387, 95-103

Calixarene-based Stationary Phases for Chromatography. G. Delahousse, R. Lavendomme, I. Jabin, V. Agasse, P. Cardinael. Curr. Org. Chem., 2015, 19, 2237-2249

2014

Crystallization of molecular systems from solution: phase diagrams, supersaturation and other basic concepts. G. Coquerel. Chem. Soc. Rev.,2014, 43 (7), 2286-2300

Crystal growth, structure, and polymorphic behavior of an ionic liquid: phthalate derivative of N-butyl,N-methylimidazolium hexafluorophosphate. C. Brandel, G. Gbabode, Y. Cartigny, C. Martin, G. Gouhier, S Petit, G. Coquerel. Chem. Mater. 2014, 26, 4151-4162

Racemic compound versus conglomerate: concerning the crystal chemistry of the triazoylketone, 1-(4-chlorophenyl)-4,4-dimethyl-2-(1H1,2,4-triazol-1-yl)pentan-3-one. R. J. Davey, G. Sadiq, C. C. S. Robin, G. Pritchard, G. Coquerel, C. Rougeot. CrystEngComm, 2014, 16, 4377-4381

Ionic co-crystals of racetams: solid-state properties enhancement of neutral active pharmaceutical ingredients via addition of Mg2+ and Ca2+ chlorides. F. Grepioni, J. Wouters, Dario Braga, S. Nanna, B. Fours, G. Coquerel, G. Longfils, S. Rome, L. Aerts, L. Quéré. CrystEngComm, 2014, Advance Article, DOI: 10.1039/C4CE00409D

A Racemic and Enantiopure Unsymmetric Diiron(III) Complex with a Chiral o-Carborane-based Pyridylalcohol Ligand:  Combined Chiroptical, Magnetic and Non Linear Optical Properties. F. Di Salvo, M. Ying Tsang, F. Teixidor, C. Viñas, J. Giner Planas, J. Crassous, N. Vanthuyne, N. Aliaga-Alcalde, E. Ruiz, G. Coquerel, S. Clevers, V. Dupray, D. Choquesillo-Lazarte, M. E. Light, M. B. Hursthouse. Chemistry: A European Journal, 2014, 20(4), 1081-1090

Effects of temperature on the polymorphism of a,w-dioctylterthiophene in thin films. C. Lercher, R. Resel, J.-Y. Balandier, C. Niebel, Y. H. Geerts, M. Sferrazza, G. Gbabode. J. Cryst. Growth, 2014, 386, 128-134

High-density octadecyl chemically bonded core-shell silica phases for high-performance liquid chromatography: comparison of microwave-assisted and classical synthetic routes, structural characterization and chromatographic evaluation. M. Mignot, A. Tchapla, O. Mercier, N. Couvrat, S. Tisse , P. Cardinael. Chromatagraphia, 2014, 77, 1577-1588

Mathematical Modelling of Chiral Symmetry Breaking towards Complete Deracemization due to Differences in Crystal Growth Kinetics. K. Suwannasang, G. Coquerel, C. Rougeot, A.E. Flood. Chem. Eng. Techn., 2014,  DOI: 10.1002/ceat.201400056

X-ray structural investigation of nonsymmetrically and symmetrically alkylated [1]benzothieno[3,2-b]benzothiophene derivatives in bulk and thin films. G. Gbabode, M. Dohr, C. Niebel, J.-Y. Balandier, C. Ruzié, P. Négrier, D. Mondieig, Y. H. Geerts, R. Resel, M. Sferrazza ACS Appl. Mater. Interfaces, 2014, 6, 13413-13421

Detection of order-disorder transition in organic solids by using Temperature Resolved Second Harmonic Generation (TR-SHG). S. Clevers, C. Rougeot, F. Simon, M. Sanselme, V Dupray, G. Coquerel. J. Mol. Structure, 2014, 1078, 61–67

Influence of the cation size on the second harmonic generation response of chiral A(VO2)2(PO4).3H2O (A = K+, NH4+ and Rb+). R. Gautier, S. Auguste, S. Clevers, V. Dupray, G. Coquerel, E. Le Fur. CrystEngComm, 2014, In Press, DOI: 10.1039/C4CE01847H

Occurrence of 1,1′-dimethyl-4,4′-bipyridinium (Paraquat) in irrigated soil of the Lake Chad Basin, Niger. M. Crampon, Y. Copard, G. Favreau, J. Raux, N. Merlet-Machour, M. Le Coz, M. Ibrahim, V. Peulon-Agasse, F. Portet-Koltalo. Environ. Sci. Pollut. R., 2014, 21(18), 10601-10613

Physical Ionic Liquid/Polysiloxane Mixtures for Tuning the Polarity and the Selectivity of the Polysiloxane Stationary Phase for GC Analysis. A. Curat, S. Tisse, A. Andrieu, N. Bar, D. Villemin, P. Cardinael. Chromatographia, 2014, 77, 1671-1681


2013


Comprehensive determination of the solid state stability of bethanechol chloride active pharmaceutical ingredient using combined analytical tools. Romain Rotival, Yohann Corvis, Yohann Cartigny, Philippe Négrier, Mathieu Marchivie, Stéphane Massip, Inès Gana, Pascale Lemoine and Philippe Espeau. Cryst Eng Comm, 2013,15, 7970-7980

Monotropic transition mechanism of m-hydroxybenzoic acid investigated by Temperature Resolved Second Harmonic Generation. Clevers, Simon; Simon, Florent; Sanselme, Morgane; Dupray, Valerie; Coquerel, Gérard. Cryst. Growth Des., 2013 vol. 13, no. 8, pp. 3697-3704

Impact of Molecular Flexibility on Double Polymorphism, Solid Solutions and chiral Discrimination during Crystallization of Diprophylline Enantiomers. C. Brandel, Y. Amharar, J. Rollinger, U. Griesser, Y. Cartigny, S. Petit, G. Coquerel. J. Molecular Pharmaceutics 2013, vol. 10, issue 10, 3850-3861

Using Programmed Heating-Cooling Cycles with Racemization in Solution for Complete Symmetry Breaking of a Conglomerate Forming System. Suwannasang  Kittisak, Flood Adrian, Rougeot Celine, Coquerel Gérard. Cryst. Growth Des., 2013 13, n°8, 3498-3504

Effect of the second coordination sphere on new contrast agents based on cyclodextrin scaffolds for MRI signals. H. Idriss, F. Estour, I. Zgani, C. Barbot, A. Biscotti, S. Petit, C. Galaup, M. Hubert-Roux, L. Nicol, P. Mulder, G. Gouhier. RSC Advances, 2013, 3, 4531-4534

Preparative resolution of (±)-Bis-tetralone by means of Auto-Seeded Preferential Crystallization Induced by Solvent Evaporation (ASPreCISE). Mahieux Julien, Sanselme Morgane, Harthong Steven, Melan Caroline, Aronica Christophe, Guy  Laure, Coquerel Gérard. Cryst. Growth Des., 2013 13(8), 3621-3631

Combining zone melting and preparative chromatography to purify Phenanthrene. Nicolas Couvrat, Antoine Burel, Séverine Tisse, Yohann Cartigny, Gérard Coquerel. Journal of Thermal Analysis and Calorimetry 2013, 112, 293-300,

Temperature resolved second harmonic generation to probe the structural purity of m-hydroxybenzoic acid. S. Clevers, F. Simon, V. Dupray and G. Coquerel. Journal of Thermal Analysis and Calorimetry, 2013,112, 271-277

Characterization of the transition between the monohydrate and the anhydrous citric acid. A. Lafontaine, M. Sanselme, Y. Cartigny, P. Cardinael and G. Coquerel. Journal of Thermal Analysis and Calorimetry, 2013,112,307-312

Thermal growth of organic supramolecular crystals with screw dislocations. A. Dhotel, L. Delbreilh, B. Youssef, J. Jiang, G. Coquerel, J-M Saiter, L. Tan. Journal of Thermal Analysis and Calorimetry, 2013,112, 301-305

The incorporation of calix[6]arene and cyclodextrin derivatives into sol–gel for the preparation of stationary phases for gas chromatography.G. Delahousse, V. Peulon-Agasse, J.-C. Debray, M. Vaccaro, G. Cravotto, I. Jabin, P. Cardinael. J. Chromatogr. A, 2013, 1318, 207– 216

Access to single crystals of (±)-Form IV of Modafinil by crystallization in gels; comparisons between (±)-Forms I, III and IV and (-)-Form I. J. Maheux, M. Sanselme and G. Coquerel. Crystal Growth and Design, 2013, 13 (2), pp 908-917

The influence of alkoxy substitutions on the properties of diketopyrrolopyrrole-phenyl copolymers for solar cells. Z. George, R. Kroon, R. Gehlhaar, G. Gbabode, A. Lundin, S. Hellström, C. Müller, Y. Geerts, P. Heremans, M. R. Andersson. Materials, 2013, 6, 3022-3034

2012

Pre-formulation of an oral cyclosporine free of surfactant Taher Boukhris, Malika Lahiani-Skiba, Damien Martins and Mohamed Skiba. Journal of Inclusion Phenomena and Macrocyclic Chemistry DOI 10.1007/s10847-012-0189-6, published online on June 20, 2012

Mixed Crystals in Chiral Organic Systems: A Case Study on (R)- and (S)-Ethanolammonium 3-Chloromandelate Authors: N. V. Taratin, H. Lorenz, E. N. Kotelnikova, A. E. Glikin, A. Galland, V. Dupray, G. Coquerel, and A. Seidel-Morgenstern. Crystal Growth and Design, 2012, 12 (12), pp 5882-5888

Hetero-DielseAlder reactions of perfluoroalkyl thioamides with electron-rich 1,3-dienes: synthesis of new 2-aminosubstituted-3,6- dihydro-2H-thiopyrans and related compounds Oleksandr S. Kanishchev, Morgane Sanselme, Jean-Philippe Bouillon. Tetrahedron 69 (2013) 1322e1336

Hybrid Mechanism in Chiral Discrimination Induced by Crystallization of Supramolecular Compounds Amharar Y., Grandeury A., Sanselme M., Petit S., Coquerel, G. J. Phys. Chem. B, 2012,116, 6027-6040

Synthesis of phosphoantigens: scalable accesses to enantiomers of BrHPP and studies on N-HDMAPP synthesis D. Brégeon, L. Ferron, A. Chrétien, F. Guillen, V. Zgonnik, M. Rivaud, M-R Mazières, G. Coquerel, Ch. Belmant, J-C Plaquevent. Bioorganic & Medicinal Chemistry Letters, 22, 2012, 5807-5810

Structural investigation on sodium-2-keto-L-gulonate-monohydrate S.S. Dette, M. Sanselme, T. Stelzer, L. Renou, M.J. Jones, N. Couvrat, G. Coquerel, J. Ulrich. Journal of Molecular Structure 1020 (2012) 121-126

Physical transformations of the active pharmaceutical ingredient BN83495: enantiotropic and monotropic relationships. Access to several polymorphic form by using various solvation-desolvation processes. D. Martins, M. Sanselme, O. Houssin, V. Dupray, M.N. Petit, D. Pasquier, C. Diolez and G. Coquerel. CrystEngComm, 2012, 14 (7), 2507 - 2519, (Special issue on pharmaceuticals)

Crystal structure of a hybrid salt-cocrystal and its resolution by preferential crystallization: ((±)trans-N,N'-dibenzyldiaminocyclohexane)(2,3-dichlorophenylaceticacid)4 J. Mahieux, S. Gonella, M. Sanselme and G. Coquerel. CrystEngComm, 2012, 14 (1), 103 - 111

Design and scalable synthesis of new chiral selectors. Part 2: Chiral Ionic Liquids Derived from Diaminocyclohexane and Histidine V. Zgonnik, S. Gonella, M-R Mazires, F. Guillen, G. Coquerel, N. Saffon and J-C. Plaquevent. Org. Process Res. Dev. 2012, 16, 277-285

Spotting a Conglomerate is just halfway to achieving a preparative resolution by Preferential Crystallization S. Gonella, J. Mahieux, M. Sanselme and G. Coquerel. Org. Process Res. Dev. 2012, 16, 286-293

Incidence of crystal growth conditions on the formation of macroscopic liquid inclusions in Ciclopirox crystals A. Waldschmidt, V. Dupray, B. Berton, N. Couvrat, S. Petit, G. Coquerel.  J. Cryst. Growth, 2012, Vol. 342, 1, 72-79

Influence of amino acid moiety accessibility on the chiral recognition of cyclodextrin-amino acid mixed selectors in enantioselective gas chromatography.
O. Stephany, S. Tisse, G. Coadou, J.-P. Bouillon, V. Peulon-Agasse, P. Cardinael. J. Chromatogr. A, 2012, 1270, 254-261

The prolongation of the lifespan of rats by repeated oral administration of [60]fullerene. B. Tarek, B. Fanchon, G. Najla, N. Leila, A. Manef, K. Abdelhamid, S. Henri, M. Fathi. Biomaterials 2012, 33(19), 4936-4946


Biomimetic layer-by-layer templates for calcium phosphate biomineralization.K. Abdelkebir, S. Morin-Grognet, F. Gaudière, G. Coquerel, B. Labat, H. Atmani, G. Ladam. Acta Biomaterialia, 2012, 8 (9), 3419-3428

2011

Protein-Triggered Instant Disassembly of Biomimetic Layer-by-Layer Films K. Abdelkebir, F. Gaudiere, S. Morin-Grognet, G. Coquerel, H. Atmani, B. Labat, and G. Ladam Langmuir 2011, 27, 14370-14379

Impact of gas composition in the mother liquor on the formation of macroscopic inclusions and crystal growth rates. Case study with Ciclopirox crystals A Waldschmidt, N. Couvrat, B. Berton, V. Dupray, S. Morin, S. Petit, G. Coquerel. Cryst. Growth Des., 2011, 11 (6), 2463-2470

About aged heterogeneous liquid inclusions inside organic crystals in relation to crystal formation, structure and morphology A. Waldschmidt, I. Rietveld, N. Couvrat, V. Dupray, M. Sanselme, B. Berton, B. Nicolai, N. Mahé, S. Petit, R. Céolin, G. Coquerel. Cryst. Growth Des., 2011, 11 (6), 2580-2587

Crystal structures, dehydration mechanism and chiral discrimination in the solid state of a hydantoin derivative Y. Amharar, S. Petit, M. Sanselme, Y. Cartigny, M.-N. Petit, G. Coquerel. Cryst. Growth Des., 2011, 11 (6), 2453-2462

Formation of crystalline hollow whiskers as relics of organic dissipative structures D. Martins, T. Stelzer, J. Ulrich, G. Coquerel. Cryst. Growth Des., 2011, 11 (7), 3020-3026

Design and scalable synthesis of new chiral selectors. Part 1: Synthesis and characterization of a new constrained cyclopeptide from unnatural bulky amino acids L. Ferron, F. Guillen, S. Coste, G. Coquerel, P. Cardinael, J. Schwartz, J.-M. Paris, J.-C. Plaquevent. Tetrahedron, 2011, 67 (33), 6036-6044

Evidence of Different Growth Regimes Coexisting within Biomimetic Layer-by-Layer Films Khalil Abdelkebir, Fabien Gaudière, Sandrine Morin-Grognet, Gérard Coquerel, Béatrice Labat, Hassan Atmani, Guy Ladam. Soft Matter 2011, 7, 9197-9205

Efficient preparation of optically pure enantiomers of alpha-aryl-alpha-trifluoromethylglycines via auto seeded programmed polythermic preferential crystallization of 5-aryl-5-trifluoromethylhydantoins. Martin T., Massif C., Wermester N., Linol J., Tisse S., Cardinaël P., Coquerel G., Bouillon J. P. Tetrahedron Asymmetry 22, 2011, 12­21

Racemizable systems crystallizing as conglomerate and spontaneous symmetry breaking. Gonella S., Levilain G., Coquerel G. J. Therm. Anal. & Calor.  2011 103:125129

Second Generation Calix[6]trenamides – Highly Selective Graftable Receptors for Neutral Guests and Contact Ion Pairs , A. Lascaux, G. Delahousse, J. Ghostin, J.-P. Bouillon, I. Jabin Eur. J. Org. Chem. 2011, 27, 5272

Recent applications of comprehensive two-dimensional gas chromatography to environmental matrices. (book chapter), P. Cardinael, A. Bruchet , V. Peulon-Agasse, in Gas chromatography book 3, 2011 Intech ISBN 979-953-307-737-5, 437-460

New and old NMR experiments for the resonance assignment of complex oligosaccharides – application to a cyclodextrin derivative B. Plainchont, A. Martinez, S. Tisse, J.-P. Bouillon, F. Pilard, J.-M. Wieruszeski, G. Lippens, D. Jeannerat, J.-M. Nuzillard, Magnetic Resonance in Chemistry, 49(12), 2011, 781-787

2010

Fascinating control of crystalline microstructures. Dette S. S., Stelzer T., Jones M. J., Coquerel G., Ulrich J. Chem. Eng. Res. Des. 2010, 88, 1158-62

Cristallisation et analyse structurale de composés supramoléculaires.  Amharar Y., Grandeury A., Sanselme M., Petit S., Coquerel G. Ann. Pharm. Franç. 2010, 68, (4), 212-17

Pitfalls and rewards of preferential crystallization. Levilain G., Coquerel G. CrystEngComm. Highlight 2010, 12, (7), 1983-92

Preparative resolution of (+/-) trans-1,2-diaminocyclohexane by means of preferential crystallization of its citrate monohydrate. Galland A.,Dupray V., Lafontaine A., Berton B., Sanselme M., Atmani H., Coquerel G. Tetrahedron Asymmetry 2010, 21, (18), 2212-17

Resolution of (+/-) Imeglimin - 2,4-dichlorophenylacetate methanol solvate by preferential crystallization. Wacharine S., Levilain G., Dupray V., Coquerel G. Org. Process Res. Dev. 2010, 14, (6), 1358-1363

An alternative scheme for the multiplexed acquisition of 1D and 2D NMR spectra. Journal of Magnetic Resonance, 2010, 206, 68-73

Synthesis, structure and affinity of novel 3-alkoxy-1,2-dihydro-3H-1,4-benzodiazepin-2-ones for CNS central and peripheral benzodiazepine receptors Andronati Sergey; Semenishyna Ekaterina; Pavlovsky Victor; Simonov Yuriy; Makan Svetlana; Boyko Irina; Burenkova Natalya; Gdaniec Maria; Cardinael Pascal; Bouillon Jean-Philippe; et al, European journal of medicinal chemistry 45(4), 2010, 1346-51

Convex hull: A new method to determine the separation space used and to optimize operating conditions for comprehensive two-dimensional gas chromatography Semard Gaelle; Peulon-Agasse, Valerie; Bruchet, Auguste; Bouillon, Jean-Philippe; Cardinael Pascal, Journal of Chromatography, A 1217(33), 2010, 5449-5454

2009

Dédoublement de molécules pharmaceutiques chirales par cristallisation préférentielle. Coquerel, G. Annales Pharmaceutiques françaises 2009, 67, 256-64

Characterization of macro defects inside single crystals of ciclopirox. Couvrat N., Blier A.-S., Berton B., Cartigny Y., Dupray V., Coquerel G. Crystal Growth & Design 2009, 9, (6), 2719-24

Structural and physico-chemical characterization of a solid solution produced by antisolvent crystallization of a new phosphoantigen. Descamps G., Cartigny Y., Sanselme M., Petit M.-N., Petit S., Aubin E., Coquerel G.Crystal Growth & Design 2009 9, (9), 3910-17

Two concomitant polymorphs of 1,2-naphtoquinone-2-semicarbazone. Dureisseix V., Sanselme M., Robin Y., Coquerel G. Crystal Growth & Design 2009, 9, (8), 3438-43

Spotting conglomerates by second harmonic generation. Galland A., Dupray V., Berton B., Morin S., Sanselme M., Atmani H., Coquerel G. Crystal Growth & Design 2009, 9, (6), 2713-18

Mechanism of hydration and dehydration of ciclopirox olamine (1:1). Renou L., Coste S., Cartigny Y., Petit M.-N., Vincent C., Schneider J.-M., Coquerel G. Crystal Growth & Design 2009, 9, (9), 3918-27

Structural studies of several solvated potassium salts of tenetoprazole crystallizing as conglomerates. Tauvel G., Sanselme M., Coste-LecomteS., Petit S., Coquerel G. J. Mol. Struct. 2009, 936, 60-66

Attrition-enhanced preferential crystallization combined with racemization leading to redissolution of the antipode nuclei. Levilain G., Rougeot C., Guillen F., Plaquevent J.-C., Coquerel G. Tetrahedron: Asymmetry 2009, 20, 2769-71

The resolution of 2-Hydroxy-5, 5-dimethyl-4-phenyl-1, 3, 2-dioxaphosphorinan 2-Oxide(Phencyphos) by Preferential Crystallization. Leeman M., Querniard F., Vries T. R., Kaptein B., Kellog R. M. Org. Process Res. Dev., 2009, 13, (6), 1379-1381

Concomitant Dehydration Mechanisms in Single Crystals of Trehalose. Dupray V., Berton B., Ossart S., Atmani H., Petit M.-N., Coquerel G. Carbohyd. Res. 2009,344, 2539-46

Mono-2, 3 or 6-hydroxy methylated β-cyclodextrin (eicosa-O-methyl-β-cyclodextrin) isomers as chiral stationary phases for capillary GC Cousin, Herve; Peulon-Agasse, Valerie; Combret, Jean-Claude; Cardinael, Pascal, Chromatographia 69(9-10), 2009, 911-922

(L)- or (D)-valine tert-butylamide grafted on permethylated beta-cyclodextrin derivatives as new mixed binary chiral selectors: versatile tools for capillary gas chromatographic enantioseparation Stephany O; Dron F; Tisse S; Martinez A; Nuzillard J-M; Peulon-Agasse V; Cardinael P; Bouillon J-P, Journal of chromatography. A 1216(18), 2009, 4051-62

2008

Preferential crystallization (AS3PC mode) of modafinic acid: an example of productivity enhancement by addition of a non-chiral base. Wermester N., Lambert O., Coquerel G. CrystEngComm 2008, 10, 724-733

Influence of ageing, grinding and preheating on the thermal behaviour of -lactose monohydrate. Garnier S., Petit S., Mallet F., Petit M.-N. Lemarchand D.; Coste S., Lefebvre J., Coquerel G. Int. J. Pharm. 2008, 361, 131-140

Use of comprehensive two-dimensional gas chromatography for the broad screening of hazardous contaminants in urban wastewaters Semard, Gaelle; Bruchet, Auguste; Cardinael, Pascal; Bouillon, Jean-Philippe,Water Science and Technology 57(12), 2008, 1983-1989

 

Study of the signifiance of comprehensive two-dimensional gas chromatography for analysis of complex environmental matrices G.Sémard, A. Bruchet, P. Cardinaël, V. Peulon-Agasse, Spectra Anal. 37(261), 2008, 29-33

Separation and Quantitative Analysis of Alkyl Sulfate Ethoxymers by HPLC  J. Morvan, M. Hubert-Roux, V. Agasse, P. Cardinaël, F. Barbot, G. Decock, J.-P. Bouillon, J.Chromatogr. Sci. 46(10), 2008, 876-82

Metastable amphiphilic hydrogels based on crosslinked carboxymethylpullulan Legros, Melanie; Cardinael, Pascal; Dulong, Virginie; Picton, Luc; Le Cerf, Didier, Polymer Journal (Tokyo, Japan) 40(3), 2008, 233-240

Indirect and direct approaches in the synthesis of a new mono-6-O-benzyl methylated γ-cyclodextrin as chiral selector for enantioselective gas chromatography Chaise, Thomas; Cardinael, Pascal; Tisse, Severine; Combret, Jean-Claude; Bouillon, Jean-Philippe, Tetrahedron:

Desymmetrization of a meso-allylic acetal by enantioselective conjugate elimination Xu Ling; Regnier Thomas; Lemiegre Loic; Cardinael Pascal; Combret Jean-Claude; Bouillon Jean-Philippe; Blanchet Jerome; Rouden Jacques; Harrison-Marchand Anne; Maddaluno Jacques, Organic letters 10(5), 2008, 729-32

2007

Gas Vacuoles Formation during the Dehydration of Trehalose Dihydrate: a Raman Microspectroscopy Approach B. Berton, V. Dupray, H. Atmani et G. Coquerel. J. Therm. Anal. & Calor. 2007

Chiral Discrimination in Host-Guest Supramolecular Complexes. Understanding Enantioselectivity and Solid Solution Behaviors by Using Spectroscopic Methods and Chemical Sensors A. Grandeury, E. Condamine, L. Hilfert, G. Gouhier, S. Petit et G. Coquerel. J. Phys. Chem. B 2007, 111, (25), 7017-7026.

Influence of high energy milling on the kinetics of the polymorphic transition from the monoclinic form to the orthorhombic form of: (±)5-methyl-5-(4'-methylphenyl)hydantoin J. Linol et G. Coquerel. J. Therm. Anal. & Calor. 2007, 90,( 2), 367-370.

 

Inversion of the relative stability between two polymorphic forms of (±) modafinil under dry high energy milling: comparisons with results obtained under wet high energy milling. J. Linol, T. Morelli, M.-N. Petit, G. Coquerel. Crystal Growth & Design 2007, 7, (9), 1608-1611.

 

Absolute configuration and structural features of R207910, a novel anti-tuberculosis agent. S. Petit, G. Coquerel, C. Meyer, J. Guillemont. J. J. Mol. Struct. 2007, 837, 252-256.

 

Role of structural and macrocrystalline factors in the desolvation behaviour of cortisone acetate solvates S. Petit, F. Mallet, M.-N. Petit et G. Coquerel J. Therm. Anal. & Calor. 2007, 90, (1), 39-47.

 

Synthesis and X-ray structural studies of the dextro-rotatory enantiomer of methyl -5(4,5,6,7-tetrahydro(3,2-c)thieno pyridyl) (2-chlorophenyl)-acetate isopropylsulfate L. Renou, S. Coste et G. Coquerel Journal of Molecular Structure 2007, 827, (1-3), 108-113.

 

Preferential crystallization in an unusual case of conglomerate with partial solid solutions N. Wermester, E. Aubin, M. Pauchet, S. Coste, et G. Coquerel Tetrahedron : Asymmetry 2007, 18, 821-831.

 

Polar dissolution and regrowth of -modafinil twins grown in gels. M. Pauchet et G. Coquerel Crystal Growth & Design 2007, 7, (9), 1612-1614.

 

Study of the quaternary system (+) and (-)5-phenyl-5-trifluroromethyl-imidazolidine-2,4-dione / (-)1-phenyl-ethylamine / Ethanol  at 20°C under atmospheric pressure. F. Querniard, J. Linol, Y. Cartigny et G. Coquerel J. Therm. Anal. & Calor. 2007.

 

Chiral discrimination at the solid state of the methyl 2-(diphenylmethylsulfinil)acetate L. Renou, T. Morelli, S. Coste, M.-N. Petit, B. Berton, J.-J. Malandain et G. Coquerel Crystal Growth & Design 2007, 7, (9), 1599-1607

 

Design, synthesis and structural analysis of new macrocycles containing dispiro-1,3-dioxane units. Florian, Maria Carmen; Grosu, Ion; Condamine, Eric; Toupet, Loic; Ramondenc, Yvan; Ple, Gerard; Cardinael, Pascal, Supramolecular Chemistry 19(6), 2007, 383-392

2006

Capillary gas chromatography properties of three new mono-ester permethylated b-cyclodextrin derivatives S. Tisse, V. Peulon-Agasse, P. Cardinael, J. -P. Bouillon, J. -C. CombretAnal. Chim. Acta, 2006

Characterization of the ethoxylated fatty chains of anionic surfactants and determination of residual ethoxylated fatty alcohols J. Morvan, M. Saluden, V. Agasse, F. Barbot, P. Cardinael, J -P. Bouillon, G. Decock Anal. Bioanal. Chem., 2006

Characterization of the ethoxylated fatty chains of anionic surfactants and determination of residual ethoxylated fatty alcohols.Julien Morvan, Magali Saluden, Valerie Agasse, Florence Barbot, Pascal Cardinael, Jean-Philippe Bouillon, Gautier Decock.Anal. Bioanal.Chem., 2006, 384, 1409-1415.

Capillary gas chromatography properties of three new mono-ester permethylated Severine Tisse, Valerie Peulon-Agasse, Pascal Cardinael, Jean-Philippe Bouillon, Jean-Claude Combret. Anal. Chim. Acta, 2006, 560, 207-217.

Thermodynamic predictions of physical properties - Prediction of solid solutions in molecular solutes exhibiting polymorphism G. Coquerel Chem. Eng. Technol. 2006, 29, 182-186


2005

Enantioselective and diastereoselective synthesis of fluorinated dipeptides by late electrophilic fluorination B. Mohar, D. Sterk, L. Ferron, D. Cahard Tetrahedron Letters 2005, 46, 5029-5031 (+ corrigendum)

Polarizing a Hydrophobic Cavity for the Efficient Binding of Organic Guests: the Case of Calix[6]tren, a Highly Efficient and Versatile Receptor for Neutral or Cationic Species U. Darbost, M.-N. Rager, S. Petit, I. Jabin, O. Reinaud J. Am. Chem. Soc. 2005, 127, 8517-8525

New Synthesis of (Z,E)-2,7-bis(4-cyanobenzylidene)cycloheptan-1-one under Stereospecific Constraints Induced by Host-Guest Interactions A. Grandeury, S. Petit, S. Coste, G. Coquerel, C. Perrio, G. Gouhier Chem. Commun. 2005, 4007-4009

Ring fission of chiral cyclic acetals plus intramolecular [4+2] cycloaddition: a sequential access to medium-size lactones. Application to the synthesis of carbasugars L. Lemiègre, R. L. Stevens, J.- C. Combret, J. Maddaluno Org. Biomol. Chem. 2005, 3, 1308-1318

A convenient access to aminals in aprotic media and direct synthesis of a-N-alkyl and N,N-dialkylaminophosphonates under Zn-Montmorillonite catalysis A. Atmani, O. Bensaid, C. Malhiac, J.-C. Combret J. Soc. Alger. Chim. 2005, 15, 77-82

Evaluation of C-trialkylsilyl enol and thioenol ethers as intermediates in the synthesis of acylsilanes C. Hammaecher, I. Ouzanne, Charles Portella, J.-P. Bouillon Tetrahedron 2005, 61, 657-663

Perfluoroketene dithioacetals : versatile building blocks towards trifluoromethyl heterocycles C. Portella, J. -P. Bouillon ACS Symposium Series # 911, Soloshonok, V. A. Ed., Oxford University Press / American Chemical Society, Washington D.C. 2005, Chapitre 12, 232-247

New intra-intermolecular criss-cross cycloaddition of unsymmetrical allenylazines with alkynes leading to three fused five-membered heterocycles S. Man, M. Necas, J. -P. Bouillon, H. Baillia, D. Harakat, M. Potacek Tetrahedron 2005, 61, 2387-2393

A new strategy for the synthesis of highly functionalised fluorinated compounds by reaction of lithium dianions of carboxylic acids with perfluoroketene dithioacetals E. Sotoca, J. -P. Bouillon, S. Gil, M. Parra, C. Portella Tetrahedron 2005, 61, 4395-4402

The full evaporation technique : a promising alternative for residual solvent analysis in solid samples A. Brault, V. Peulon-Agasse, P. Cardinael, J.-C. Combret J. Separation Science 2005, 28, 380-386

2004

Resolution of the ethanolamine salt of (±) mandelic acid by using the AS3PC method : principle, application and results E. Aubin, M.N. Petit, G. Coquerel J.Phys. IV France, Proceedings of JEEP-XXX, 2004, 122,157-162

Application of the DCP model to a metastable racemate of mandelic acid M. Pauchet, G. Coquerel J.Phys. IV France, Proceedings of JEEP-XXX, 2004, 122,177-18

Peptide synthesis in room temperature ionic liquids H. Vallette, L. Ferron, G. Coquerel, A.-C. Gaumont, J.-C. Plaquevent Tetrahedron Letters 2004, 45(8), 1617-1619

Crystal growth mechanism in a solution of hollow whiskers of molecular compounds F. Mallet, S. Petit, S. Lafont, P. Billot, D. Lemarchand, G. Coquerel Crystal Growth & Design. 2004, 4(5), 965-969

Successful Application of the DCP Model in Resolving the Crystal Structure of a Metastable Polymorph of (±)-Modafinil M. Pauchet, C. Gervais, L. Courvoisier, G. Coquerel Crystal Growth & Design. 2004, 4(6), 1143-1151

Pleconaril polymorphs : crystal structures of form I and form III, evidence of the enantiotropy and assessment of the structural purity S. Coste, J-M. Schneider, M-N. Petit, G. Coquerel Crystal Growth & Design. 2004, 4(6), 1237-1244

Pentaspiranes and hexaspiranes with 1,3-dioxane or 1,3-oxathiane rings: synthesis and stereochemistry A. Terec, I. Grosu, E. Condamine, L. Breau, G. Plé, Y. Ramondenc, F.D. Rochon, V. Peulon-Agasse, D. Opris Tetrahedron 2004, 60,3173-3189

Synthesis and structural analysis of new macrocycles exhibiting 3,9-dimethyl-3,9-diaryl-2,4,8,10-tetraoxaspiro[5.5]undecane units M. Balog, I. Grosu, G. Plé, Y. Ramondenc, L. Toupet, E. Condamine, C. Lange, C. Loutelier-Bourhis, V. Peulon-Agasse, E. Bogdan Tetrahedron 2004, 60,4789-4799

Direct and convenient access to mono 3-hydroxy per-O-methylated a-cyclodextrin T. Chaise, E. Bourgeaux, P. Cardinaël, J.C. Combret Tetrahedron Letters 2004, 45, 5853-5856

Stereoselective synthesis of new classes of atropisomeric compounds through the tandem imine Michael reaction-azacyclization process. Part 2 S. Le Gac, N. Monnier-Benoit, L. Doumampouom Metoul, S. Petit, I. Jabin Tetrahedron: Asymmetry 2004, 11,139-145

A Priori Assessment of the Maximum possible entrainment effect attainable during preferential crystallization. The case of the simultaneous resolution of ( ) ephedrine and ( ) mandelic acid. F. Dufour, G. Perez, G. Coquerel Bull. Chem. Soc. Japan 2004, 77(1), 79-86

Diastereomeric resolution rationalized by phase diagrams under the actual conditions of the experimental process P. Marchand, L. Lefèbvre, F. Querniard, P. Cardinaël, G. Perez, J.J. Counioux, G. Coquerel Tetrahedron: Asymmetry 2004, 15, 2455-2465

Impact of chirality on phase diagrams and conversely relative quantification of chirality by using the binary phase diagram of enantiomers. G. Coquerel J.Phys. IV France 2004, 113, 11-15

Chiral resolution by crystallization of host-guest supramolecular complexes. A paradoxal situation with an efficient discrimination despite structural similarities A. Grandeury, L. Renou, F. Dufour, S. Petit, G. Gouhier, G. Coquerel J. Therm. Anal. & Calor. 2004, 77, 377-390


2003

Combined effect of polymorphism and process on Preferential Crystallization. Example with (±)-5-(4'-methylphenyl)5--methylhydantoin L. Courvoisier, L. Mignot, M.N. Petit, G. Coquerel Organic Process Research & Development 2003, 7 (6), 1007-1016

Conjugated elimination versus [1,2]-Wittig rearrangement of unsaturated diox(ol)anes L. Lemiègre, T. Regnier, J.C. Combret, J. Maddaluno Tet. Let., 2003, 44, 373-377

Crystallization of supramolecular complexes as an alternative route for the separation of racemic p-X-phenylethanol   A. Grandeury, S. Tisse, G. Gouhier, V. Agasse, S. Petit, G. Coquerel Chem. Eng. Technol. 2003, 26, 354-358

Solvent exchanges among molecular compounds. Two extreme cases of pharmaceutical interest   F. Mallet, S. Petit, S. Lafont, P. Billot, D. Lemarchand, G. Coquerel J. Therm. Anal. & Calor. 2003, 73, 459-471

Enantioseparation of 1-(p-bromophenyl)ethanol by crystallization of host-guest complexes with permethylated b-cyclodextrin: crystal structures and mechanisms of chiral recognition A. Grandeury, S. Petit, G. Gouhier, V. Agasse, G. Coquerel Tetrahedron: Asymmetry 2003, 14, 2143-2152

Resolution of Pasteur salts by auto-seeded preferential crystallization M.N. Petit, G. Coquerel Mendeleev Communications 2003, 13, 95-96

Selective access and full characterization of mono-acidic permethylated-cyclodextrin derivatives and their methyl esters S. Tisse, V. Peulon-Agasse, H. Oulyadi, F. Marsais, J.C. Combret Tetrahedron: Asymmetry 2003, 14, 2259-2266

 

Synthesis,NMR spectroscopic characterization and polysiloxane-based immobilization of the three regioisomeric monooctenylpermethyl- -cyclodextrins and their application in enantioselective GC H. Cousin, O. Trapp, V. Peulon-Agasse, X. Pannecoucke, L. Banspach, G. Trapp, Z. Jiang, J.-C. Combret and V. Schurig Eur. J. Org. Chem.  2003, 3273-3287

Synthesis of , -unsaturated dioxanes, dioxalanes and dioxepanes by trnasacetalisation of dimethylacetals with meso or C2-symmetrical 1,2-1,3- and 1,4-diols L. Lemiegre, F. Lesetre,J.-C. Combret, J. Maddaluno Tetrahedron, 2003, 60, 415-427

Synthesis and Structure of New Macrocycles Including Spiro-1.3-Dioxane Units Grosu, E. Bogdan, G. Plé, L. Toupet, Y. Ramondenc, E. Condamine, V. Peulon-Agasse, M. Balog Eur. J. Org. Chem., 2003,3153-3161

2002


Influence of supersaturation and structurally related additives on the crystal growth of a-lactose monohydrate S. Garnier, S. Petit, G. Coquerel J. Crystal Growth, 2002, 234, 207-219

Oscillating crystallization in solution between (+) and (-) 5-ethyl-5-methylhydantoin under the influence of stirring C. Gervais, S. Beilles, P. Cardinael, S. Petit, G. Coquerel J. Phys. Chem. B, 2002, 106 (3), 646-652

Dehydration mechanism and crystallization behaviours of lactose S. Garnier, S. Petit, G. Coquerel J. Therm. Anal. & Calor., 2002, 68, 489-502

Enantiopurification during the Crystallization of Host-Guest Supramolecular Compounds: Crystal Growth and Structural Investigations A. Grandeury, S. Tisse, V. Agasse, G. Gouhier, S. Petit, G. Coquerel Chem. Eng. Trans., 2002, 1, 813-818

Theoretical and experimental interpretation of the signals from Discontinuous Isoperibolic Thermal Analysis P. Marchand, L. Lefebvre, G. Perez, J.-J. Counioux, G. Coquerel J. Therm. Anal. & Calor., 2002, 68, 37-47

Simple Model Designed to Generate New Crystal Structures Derived from a Mother Phase. Application to Molecular Compounds C. Gervais, G. Coquerel Acta Cryst., 2002, B58, 662-672


2001

Preferential crystallisation and comparative crystal growth study between pure enantiomer and racemic mixture of a chiral molecule: 5-ethyl-5-methylhydantoin S. Beilles, P. Cardinael, E. Ndzié, S. Petit, G. Coquerel Chem. Engineer. Sci., 2001, 56, 2281-2294

Quantitative determination of straight and cyclic hydrocarbons in crystallized permethylated-b-cyclodextrin inclusion complexes by static headspace-gas chromatography. P. Cardinael, V. Peulon-Agasse, G. Coquerel, Y. Combret, J.C. Combret J. of Separation Sci., 2001, 2, 109-115

High-Performance Liquid Chromatography investigation of the enantioselectivity and mechanism of chiral recognition of new cholic acid-based stationary phases L. Vaton-Chanvrier, Y. Combret, J. C. Combret Chromatographia, 2001, 54, 31-37

Chiral recognition of binaphthyl derivatives: A chiral recognition model on the basis of chromatography, spectroscopy and molecular mechanistic calculations for the enantioseparation of 1,1'-binaphthyl derivatives on cholic acid-bonded stationary phases L. Vaton-Chanvrier, H. Oulyadi, Y. Combret, G. Coquerel, J. C. Combret Chirality, 2001, 13 (10), 668-674

Synthesis of the three isomeric mono-2, 3, or 6-hydroxy permethylated-b-Cyclodextrins and unambiguous high field NMR characterisation . H. Cousin, P. Cardinael, H. Oulyadi, X. Pannecoucke, J. C. Combret Tetrahedron: Asymmetry, 2001, 12 (1), 81-88

Characterization of crystalline complexes between heptakis(2,3,6-tri-O_methyl)-b-cyclodextrin and various alkanes or alkenes (5£C£10) P. Cardinael, V. Peulon, G. Perez, G. Coquerel, L. Toupet J. Inclusion Phenomena & Macrocycl. Chem., 2001, 39, 159-167

Influence of the process on the mechanisms and the performances of the preferential crystallization: example with (±)-5-(4-bromophenyl)-5-methylhydantoinL. Courvoisier, E. Ndzié, M.N. Petit, U. Hedtmann, U. Sprengard, G. Coquerel Chem. Let., 2001, 4, 364-365

Investigations in the reciprocal ternary system (±) 2-phenylpropionic acid / (±) a-methylbenzylamine. Impact of an unstable racemic compound on the simultaneous resolution of chiral acids and bases by preferential crystallisation F. Dufour, C. Gervais, M.-N. Petit, G. Perez, G. Coquerel J. Chem. Soc., Perkin Trans. II, 2001, (10), 2022-2036

 

Diastereoselective alkylation of 2,3,4,6-di-O-isopropylidene-2-keto-L-gulonic amides. Application to the asymmetric synthesis of 1-substituted-1,2,3,4-tetrahydroisoquinolines and 1-substituted-1,2,3,4-tetrahydro-b-carbolines S. Adam, X. Pannecoucke, J. C. Combret, J. C. Quirion J. Org. Chem., 2001, 66, 8744-8750

Solvent exchange between dimethylsulfoxide and water in the dexamethasone acetate structure F. Mallet, S. Petit, M.-N. Petit, P. Cardinael, P. Billot, S. Lafont, G. Coquerel J. Physique IV, 2001, 11, Pr10-253-259

Effect of the polymorphic form of the seeds on the preferential crystallization L. Courvoisier, C. Gervais, L. Mignot, M.-N. Petit, G. Coquerel J. Physique IV, 2001, 11, Pr10-71-77

Discontinuous Isoperibolic Thermal Analysis (DITA) applied to organic components P. Marchand, L. Lefebvre, L. Courvoisier, G. Perez, J.-J. Counioux, G. Coquerel J. Physique IV, 2001, 11, Pr10-115-122

2000

Unsaturated a-aminophosphonates : synthesis and reactivityH. Atmani, J.C. Combret, C. Malhiac, K. Mulengi Tetrahedron Letters, 2000, 41, 6045-6048

Comparaison of grafting modes for the preparation of cholic acid-based stationary phases. Influence on enantiomer separations in high performance liquid chromatography L. Vaton-Chanvrier, N. Bucaille, Y. Combret, J. C. Combret Journal of Liquid Chromatography & Related Technologies, 2000, 23, 2155-2167

General access to asymmetric g-cyclodextrins for gas chromatographic applications, by insertion of a selective modified sugar unit. E. Bourgeaux, J. C. Combret Tetrahedron: Asymmetry, 2000, 11, 20, 4189-4205

Review on the heterogeneous equilibria between condensed phases in binary systems of enantiomers G. Coquerel Enantiomer, 2000, 5, 481-498


Chapitres de livres

G. Coquerel, R. Tamura
Enantiomeric disorder
Disordered pharmaceutical materials, Wiley VCH Verlag GmbH & Co. KGaA, Weinheim, Germany, 2016, M. Descamps ed., ISBN: 978-3-527-33125-3, DOI 10.1002/9783527652693.ch5; chapter 5, pp. 135-159

G. Coquerel
Chiral Discrimination in the Solid State; Applications to Resolution and Deracemization
Advances in Organic Crystal Chemistry: Comprehensive Reviews, 2015. ISBN 978-4-431-55554-4, p 393-420, DOI 10.1007/978-4-431; chapter 20, pp 393-420

C. Viedma, G. Coquerel, P. Cintas
Crystallization of Chiral Molecules
Handbook of Crystal Growth, Elsevier 2015, Chapter 22, pp. 951-1002

P. Cardinael, H. Casablanca, V. Peulon-Agasse, A. Berthod
Sample Derivatization in Separation Science
Analytical Separation Science,2015, (Ed) J. Anderson, A. Berthod, V. Pino, A. M. Stalcup, 2015 Wiley-VCH Verlag GmbH &Co. KGaA 1725-1756


G. Coquerel
Co-crystals and beyond
Pharmaceutical Salts and Co-Crystal,  Chapter 13, pp 300-317 in, 'RSC Publishing 2012 Editors: Johan Wouters and Luc Quéré ISBN: 978-1-84973-158-4

J. Ternois, L. Ferron, G. Coquerel, F. Guillen,
J.-C. Plaquevent
New opportunities for the chemistry of Amino-Acids, Peptides and pharmaceutical compounds. In Ionic Liquids applications: Pharmaceuticals, Therapeutics and Biotechnology, Sanjay V. Malhotra ed.; 2010; Vol. 1038, pp Chapter 2, pp 13-24

G. Coquerel, D. B. Amabilino
The Nanoscale Aspects of Chirality in Crystal Growth: Structure and Heterogeneous Equilibria’ Chapter 10 in Chirality at the nanoscale, pp 305-341, 2009, Wiley VCH,i ‘Chirality at the nanoscale’ Ed. D. B. Amabilino

G. Coquerel
Preferential Crystallization
Topics in Current Chemistry (Novel Optical Resolution Technologies), ed. Springer GmbH, 2007, pp. 1-50, ISSN: 0340-1022

S. Petit, G. Coquerel
The Amorphous State
i
n Polymorphism in the Pharmaceutical Industry, Wiley 2006, Ed Hilfiker; Wiley, pp 258-282, ISBN: 978-3-527-31146-0